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Crystallographic characterization of the structure of the endohedral fullerene [Er2@C82 isomer I] with C(s) cage symmetry and multiple sites for erbium along a band of ten contiguous hexagons.

Journal of the American Chemical Society

Olmstead MM, de Bettencourt-Dias A, Stevenson S, Dorn HC, Balch AL.
PMID: 11960421
J Am Chem Soc. 2002 Apr 24;124(16):4172-3. doi: 10.1021/ja0116019.

The structure of one of the three previously separated isomers of {Er2@C82} has been determined through a single-crystal X-ray structure determination of the noncovalent adduct, {Er2@C82 Isomer I}.{CoII(OEP)}.1.4(C6H6).0.3(CHCl3). The C82 cage is identified specificlly as the Cs(82:6) isomer (one...

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Olmstead MM, de Bettencourt-Dias A, Stevenson S, et al. Crystallographic characterization of the structure of the endohedral fullerene [Er2@C82 isomer I] with C(s) cage symmetry and multiple sites for erbium along a band of ten contiguous hexagons. J Am Chem Soc. 2002;124(16):4172-3doi: 10.1021/ja0116019.
Olmstead, M. M., de Bettencourt-Dias, A., Stevenson, S., Dorn, H. C., & Balch, A. L. (2002). Crystallographic characterization of the structure of the endohedral fullerene [Er2@C82 isomer I] with C(s) cage symmetry and multiple sites for erbium along a band of ten contiguous hexagons. Journal of the American Chemical Society, 124(16), 4172-3. https://doi.org/10.1021/ja0116019
Olmstead, Marilyn M, et al. "Crystallographic characterization of the structure of the endohedral fullerene [Er2@C82 isomer I] with C(s) cage symmetry and multiple sites for erbium along a band of ten contiguous hexagons." Journal of the American Chemical Society vol. 124,16 (2002): 4172-3. doi: https://doi.org/10.1021/ja0116019
Olmstead MM, de Bettencourt-Dias A, Stevenson S, Dorn HC, Balch AL. Crystallographic characterization of the structure of the endohedral fullerene [Er2@C82 isomer I] with C(s) cage symmetry and multiple sites for erbium along a band of ten contiguous hexagons. J Am Chem Soc. 2002 Apr 24;124(16):4172-3. doi: 10.1021/ja0116019. PMID: 11960421.
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Sequential 1,3-dipolar cycloadditions in the synthesis of bis-isoxazolo substituted piperidinones.

The Journal of organic chemistry

Huang KS, Lee EH, Olmstead MM, Kurth MJ.
PMID: 10813963
J Org Chem. 2000 Jan 28;65(2):499-503. doi: 10.1021/jo991418m.

A strategy for the efficient synthesis of novel bis-isoxazolo substituted piperidinones has been developed. The protocol consists of the Michael addition of an unsaturated alkoxide to beta-nitrostyrene followed by an intramolecular nitrile oxide cycloaddition (INOC) or an intramolecular silyl...

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Huang KS, Lee EH, Olmstead MM, et al. Sequential 1,3-dipolar cycloadditions in the synthesis of bis-isoxazolo substituted piperidinones. J Org Chem. 2000;65(2):499-503doi: 10.1021/jo991418m.
Huang, K. S., Lee, E. H., Olmstead, M. M., & Kurth, M. J. (2000). Sequential 1,3-dipolar cycloadditions in the synthesis of bis-isoxazolo substituted piperidinones. The Journal of organic chemistry, 65(2), 499-503. https://doi.org/10.1021/jo991418m
Huang, et al. "Sequential 1,3-dipolar cycloadditions in the synthesis of bis-isoxazolo substituted piperidinones." The Journal of organic chemistry vol. 65,2 (2000): 499-503. doi: https://doi.org/10.1021/jo991418m
Huang KS, Lee EH, Olmstead MM, Kurth MJ. Sequential 1,3-dipolar cycloadditions in the synthesis of bis-isoxazolo substituted piperidinones. J Org Chem. 2000 Jan 28;65(2):499-503. doi: 10.1021/jo991418m. PMID: 10813963.
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Heterolytic Cleavage of the C-C Bond of Acetonitrile with Simple Monomeric Cu(II) Complexes: Melding Old Copper Chemistry with New Reactivity This work was supported by a grant from the National Science Foundation (CHE-9818492). .

Angewandte Chemie (International ed. in English)

Marlin DS, Olmstead MM, Mascharak PK.
PMID: 12404406
Angew Chem Int Ed Engl. 2001 Dec 17;40(24):4752-4754. doi: 10.1002/1521-3773(20011217)40:24<4752::aid-anie4752>3.0.co;2-l.

No abstract available.

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Marlin DS, Olmstead MM, Mascharak PK. Heterolytic Cleavage of the C-C Bond of Acetonitrile with Simple Monomeric Cu(II) Complexes: Melding Old Copper Chemistry with New Reactivity This work was supported by a grant from the National Science Foundation (CHE-9818492). . Angew Chem Int Ed Engl. 2001;40(24):4752-4754doi: 10.1002/1521-3773(20011217)40:24<4752::aid-anie4752>3.0.co;2-l.
Marlin, D. S., Olmstead, M. M., & Mascharak, P. K. (2001). Heterolytic Cleavage of the C-C Bond of Acetonitrile with Simple Monomeric Cu(II) Complexes: Melding Old Copper Chemistry with New Reactivity This work was supported by a grant from the National Science Foundation (CHE-9818492). . Angewandte Chemie (International ed. in English), 40(24), 4752-4754. https://doi.org/10.1002/1521-3773(20011217)40:24<4752::aid-anie4752>3.0.co;2-l
Marlin, Dana S., et al. "Heterolytic Cleavage of the C-C Bond of Acetonitrile with Simple Monomeric Cu(II) Complexes: Melding Old Copper Chemistry with New Reactivity This work was supported by a grant from the National Science Foundation (CHE-9818492). ." Angewandte Chemie (International ed. in English) vol. 40,24 (2001): 4752-4754. doi: https://doi.org/10.1002/1521-3773(20011217)40:24<4752::aid-anie4752>3.0.co;2-l
Marlin DS, Olmstead MM, Mascharak PK. Heterolytic Cleavage of the C-C Bond of Acetonitrile with Simple Monomeric Cu(II) Complexes: Melding Old Copper Chemistry with New Reactivity This work was supported by a grant from the National Science Foundation (CHE-9818492). . Angew Chem Int Ed Engl. 2001 Dec 17;40(24):4752-4754. doi: 10.1002/1521-3773(20011217)40:24<4752::aid-anie4752>3.0.co;2-l. PMID: 12404406.
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Cation-controlled self-assembly of a hexameric europium wheel.

Journal of the American Chemical Society

Bretonnière Y, Mazzanti M, Pécaut J, Olmstead MM.
PMID: 12148980
J Am Chem Soc. 2002 Aug 07;124(31):9012-3. doi: 10.1021/ja012177e.

The simple asymmetric tetradentate ligand 2,2':6',2' '-terpyridine-6-carboxylic acid leads to the self-assembly of the first europium nanowheel containing europium ions in two different coordination environments. Moreover the self-assembly of bis(terpyridinecarboxylate) europium species to form a hexameric wheel capable of...

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Bretonnière Y, Mazzanti M, Pécaut J, et al. Cation-controlled self-assembly of a hexameric europium wheel. J Am Chem Soc. 2002;124(31):9012-3doi: 10.1021/ja012177e.
Bretonnière, Y., Mazzanti, M., Pécaut, J., & Olmstead, M. M. (2002). Cation-controlled self-assembly of a hexameric europium wheel. Journal of the American Chemical Society, 124(31), 9012-3. https://doi.org/10.1021/ja012177e
Bretonnière, Yann, et al. "Cation-controlled self-assembly of a hexameric europium wheel." Journal of the American Chemical Society vol. 124,31 (2002): 9012-3. doi: https://doi.org/10.1021/ja012177e
Bretonnière Y, Mazzanti M, Pécaut J, Olmstead MM. Cation-controlled self-assembly of a hexameric europium wheel. J Am Chem Soc. 2002 Aug 07;124(31):9012-3. doi: 10.1021/ja012177e. PMID: 12148980.
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Eu10Mn6Sb13: a new ternary rare-Earth transition-metal Zintl phase.

Inorganic chemistry

Holm AP, Park SM, Condron CL, Olmstead MM, Kim H, Klavins P, Grandjean F, Hermann RP, Long GJ, Kanatzidis MG, Kauzlarich SM, Kim SJ.
PMID: 12870957
Inorg Chem. 2003 Jul 28;42(15):4660-7. doi: 10.1021/ic034054w.

A new transition-metal-containing Zintl compound, Eu(10)Mn(6)Sb(13), was prepared by a high-temperature Sn-flux synthesis. The structure was determined by single-crystal X-ray diffraction. Eu(10)Mn(6)Sb(13) crystallizes in the monoclinic space group C2/m with a = 15.1791(6) A, b = 19.1919(7) A, c...

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Holm AP, Park SM, Condron CL, et al. Eu10Mn6Sb13: a new ternary rare-Earth transition-metal Zintl phase. Inorg Chem. 2003;42(15):4660-7doi: 10.1021/ic034054w.
Holm, A. P., Park, S. M., Condron, C. L., Olmstead, M. M., Kim, H., Klavins, P., Grandjean, F., Hermann, R. P., Long, G. J., Kanatzidis, M. G., Kauzlarich, S. M., & Kim, S. J. (2003). Eu10Mn6Sb13: a new ternary rare-Earth transition-metal Zintl phase. Inorganic chemistry, 42(15), 4660-7. https://doi.org/10.1021/ic034054w
Holm, Aaron P, et al. "Eu10Mn6Sb13: a new ternary rare-Earth transition-metal Zintl phase." Inorganic chemistry vol. 42,15 (2003): 4660-7. doi: https://doi.org/10.1021/ic034054w
Holm AP, Park SM, Condron CL, Olmstead MM, Kim H, Klavins P, Grandjean F, Hermann RP, Long GJ, Kanatzidis MG, Kauzlarich SM, Kim SJ. Eu10Mn6Sb13: a new ternary rare-Earth transition-metal Zintl phase. Inorg Chem. 2003 Jul 28;42(15):4660-7. doi: 10.1021/ic034054w. PMID: 12870957.
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Solid-phase synthesis of an isoxazolinopyrrole library.

Journal of combinatorial chemistry

Hwang SH, Olmstead MM, Kurth MJ.
PMID: 14714998
J Comb Chem. 2004 Jan-Feb;6(1):142-8. doi: 10.1021/cc034023w.

A four-step solid-phase synthesis of isoxazolinopyrroles 8 that employs an acid-labile 2-(4-formyl-3-methoxyphenoxy)ethyl polystyrene HL resin 1 is reported. Resin-bound vinyl sulfone 5 is obtained by DIC coupling with acid 4, which was in turn synthesized in solution phase by...

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Hwang SH, Olmstead MM, Kurth MJ. Solid-phase synthesis of an isoxazolinopyrrole library. J Comb Chem. 2004;6(1):142-8doi: 10.1021/cc034023w.
Hwang, S. H., Olmstead, M. M., & Kurth, M. J. (2004). Solid-phase synthesis of an isoxazolinopyrrole library. Journal of combinatorial chemistry, 6(1), 142-8. https://doi.org/10.1021/cc034023w
Hwang, Sung Hee, et al. "Solid-phase synthesis of an isoxazolinopyrrole library." Journal of combinatorial chemistry vol. 6,1 (2004): 142-8. doi: https://doi.org/10.1021/cc034023w
Hwang SH, Olmstead MM, Kurth MJ. Solid-phase synthesis of an isoxazolinopyrrole library. J Comb Chem. 2004 Jan-Feb;6(1):142-8. doi: 10.1021/cc034023w. PMID: 14714998.
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Convenient synthesis of aluminum and gallium phosphonate cages.

Inorganic chemistry

Samanamu CR, Olmstead MM, Montchamp JL, Richards AF.
PMID: 18366160
Inorg Chem. 2008 May 05;47(9):3879-87. doi: 10.1021/ic800023d. Epub 2008 Mar 26.

The reactions of AlCl 3.6H 2O and GaCl 3 with 2-pyridylphosphonic acid (2PypoH 2) and 4-pyridylphosphonic acid (4PypoH 2) afford cyclic aluminum and gallium phosphonate structures of [(2PypoH) 4Al 4(OH 2) 12]Cl 8.6H 2O ( 1), [(4PypoH) 4Al 4(OH...

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Samanamu CR, Olmstead MM, Montchamp JL, et al. Convenient synthesis of aluminum and gallium phosphonate cages. Inorg Chem. 2008;47(9):3879-87doi: 10.1021/ic800023d.
Samanamu, C. R., Olmstead, M. M., Montchamp, J. L., & Richards, A. F. (2008). Convenient synthesis of aluminum and gallium phosphonate cages. Inorganic chemistry, 47(9), 3879-87. https://doi.org/10.1021/ic800023d
Samanamu, Christian R, et al. "Convenient synthesis of aluminum and gallium phosphonate cages." Inorganic chemistry vol. 47,9 (2008): 3879-87. doi: https://doi.org/10.1021/ic800023d
Samanamu CR, Olmstead MM, Montchamp JL, Richards AF. Convenient synthesis of aluminum and gallium phosphonate cages. Inorg Chem. 2008 May 05;47(9):3879-87. doi: 10.1021/ic800023d. Epub 2008 Mar 26. PMID: 18366160.
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Terphenyl ligand stabilized lead(II) derivatives: steric effects and lead-lead bonding in diplumbenes.

Inorganic chemistry

Hino S, Olmstead M, Phillips AD, Wright RJ, Power PP.
PMID: 15530084
Inorg Chem. 2004 Nov 15;43(23):7346-52. doi: 10.1021/ic049174y.

The reaction of PbBr(2) with the lithium reagents LiC(6)H(3)-2,6-(C(6)H(3)-2,6-Pr(i)(2))(2) (LiArPr(i)(2)) and Et(2)O.LiC(6)H(3)-2,6-(2,6-Pr(i)-4-Bu(t)C(6)H(2))(2) (Et(2)O.LiArPr(i)(2)Bu(t)) furnished the bromide bridged organolead(II) halides [Pb(mu-Br)ArPr(i)(2)](2) (1) and[Pb(mu-Br)ArPr(i)(2)Bu(t)](2) (2) as orange crystals. Treatment of 1 with a stoichiometric amount of methylmagnesium bromide resulted in the...

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Hino S, Olmstead M, Phillips AD, et al. Terphenyl ligand stabilized lead(II) derivatives: steric effects and lead-lead bonding in diplumbenes. Inorg Chem. 2004;43(23):7346-52doi: 10.1021/ic049174y.
Hino, S., Olmstead, M., Phillips, A. D., Wright, R. J., & Power, P. P. (2004). Terphenyl ligand stabilized lead(II) derivatives: steric effects and lead-lead bonding in diplumbenes. Inorganic chemistry, 43(23), 7346-52. https://doi.org/10.1021/ic049174y
Hino, Shirley, et al. "Terphenyl ligand stabilized lead(II) derivatives: steric effects and lead-lead bonding in diplumbenes." Inorganic chemistry vol. 43,23 (2004): 7346-52. doi: https://doi.org/10.1021/ic049174y
Hino S, Olmstead M, Phillips AD, Wright RJ, Power PP. Terphenyl ligand stabilized lead(II) derivatives: steric effects and lead-lead bonding in diplumbenes. Inorg Chem. 2004 Nov 15;43(23):7346-52. doi: 10.1021/ic049174y. PMID: 15530084.
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A pirouette on a metallofullerene sphere: interconversion of isomers of N-tritylpyrrolidino I(h) Sc3N@C80.

Journal of the American Chemical Society

Cai T, Slebodnick C, Xu L, Harich K, Glass TE, Chancellor C, Fettinger JC, Olmstead MM, Balch AL, Gibson HW, Dorn HC.
PMID: 16683814
J Am Chem Soc. 2006 May 17;128(19):6486-92. doi: 10.1021/ja0601843.

The pure I(h) isomer of Sc3N@C80 was allowed to react with N-triphenylmethyl-5-oxazolidinone via the corresponding azomethine ylide. The reaction results in the formation of two monoadducts; one (1b) is the kinetic product, and the other (1a) is thermodynamically more...

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Cai T, Slebodnick C, Xu L, et al. A pirouette on a metallofullerene sphere: interconversion of isomers of N-tritylpyrrolidino I(h) Sc3N@C80. J Am Chem Soc. 2006;128(19):6486-92doi: 10.1021/ja0601843.
Cai, T., Slebodnick, C., Xu, L., Harich, K., Glass, T. E., Chancellor, C., Fettinger, J. C., Olmstead, M. M., Balch, A. L., Gibson, H. W., & Dorn, H. C. (2006). A pirouette on a metallofullerene sphere: interconversion of isomers of N-tritylpyrrolidino I(h) Sc3N@C80. Journal of the American Chemical Society, 128(19), 6486-92. https://doi.org/10.1021/ja0601843
Cai, Ting, et al. "A pirouette on a metallofullerene sphere: interconversion of isomers of N-tritylpyrrolidino I(h) Sc3N@C80." Journal of the American Chemical Society vol. 128,19 (2006): 6486-92. doi: https://doi.org/10.1021/ja0601843
Cai T, Slebodnick C, Xu L, Harich K, Glass TE, Chancellor C, Fettinger JC, Olmstead MM, Balch AL, Gibson HW, Dorn HC. A pirouette on a metallofullerene sphere: interconversion of isomers of N-tritylpyrrolidino I(h) Sc3N@C80. J Am Chem Soc. 2006 May 17;128(19):6486-92. doi: 10.1021/ja0601843. PMID: 16683814.
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Metal-metal interactions in thallium(I)/platinum(II) compounds involving a chelating dicarbene and various auxiliary ligands.

Inorganic chemistry

Stork JR, Olmstead MM, Fettinger JC, Balch AL.
PMID: 16411723
Inorg Chem. 2006 Jan 23;45(2):849-57. doi: 10.1021/ic051252+.

Reaction of Tl(I)NO(3) and (C(4)H(10)N(4))Pt(II)(mnt) or (C(4)H(10)N(4))Pt(II)(dmg-H) [mnt = maleonitriledithiolate, dmg-H = dimethylglyoximate dianion] in dilute, aqueous KOH yielded adducts of Tl(I) and the conjugate bases of the platinum(II) compounds. The compound Tl(I)[(C(4)H(9)N(4))Pt(II)(dmg-H)].5H(2)O forms as dimers with close Tl(I)...Pt(II)...

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Stork JR, Olmstead MM, Fettinger JC, et al. Metal-metal interactions in thallium(I)/platinum(II) compounds involving a chelating dicarbene and various auxiliary ligands. Inorg Chem. 2006;45(2):849-57doi: 10.1021/ic051252+.
Stork, J. R., Olmstead, M. M., Fettinger, J. C., & Balch, A. L. (2006). Metal-metal interactions in thallium(I)/platinum(II) compounds involving a chelating dicarbene and various auxiliary ligands. Inorganic chemistry, 45(2), 849-57. https://doi.org/10.1021/ic051252+
Stork, Jay R, et al. "Metal-metal interactions in thallium(I)/platinum(II) compounds involving a chelating dicarbene and various auxiliary ligands." Inorganic chemistry vol. 45,2 (2006): 849-57. doi: https://doi.org/10.1021/ic051252+
Stork JR, Olmstead MM, Fettinger JC, Balch AL. Metal-metal interactions in thallium(I)/platinum(II) compounds involving a chelating dicarbene and various auxiliary ligands. Inorg Chem. 2006 Jan 23;45(2):849-57. doi: 10.1021/ic051252+. PMID: 16411723.
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THE MUCOID PHASE OF STREPTOCOCCUS HEMOLYTICUS.

Science (New York, N.Y.)

Dawson MH, Olmstead M.
PMID: 17789304
Science. 1934 Sep 28;80(2074):296-7. doi: 10.1126/science.80.2074.296.

No abstract available.

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Dawson MH, Olmstead M. THE MUCOID PHASE OF STREPTOCOCCUS HEMOLYTICUS. Science. 1934;80(2074):296-7doi: 10.1126/science.80.2074.296.
Dawson, M. H., & Olmstead, M. (1934). THE MUCOID PHASE OF STREPTOCOCCUS HEMOLYTICUS. Science (New York, N.Y.), 80(2074), 296-7. https://doi.org/10.1126/science.80.2074.296
Dawson, M H, and Olmstead, M. "THE MUCOID PHASE OF STREPTOCOCCUS HEMOLYTICUS." Science (New York, N.Y.) vol. 80,2074 (1934): 296-7. doi: https://doi.org/10.1126/science.80.2074.296
Dawson MH, Olmstead M. THE MUCOID PHASE OF STREPTOCOCCUS HEMOLYTICUS. Science. 1934 Sep 28;80(2074):296-7. doi: 10.1126/science.80.2074.296. PMID: 17789304.
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Interplay of supramolecular organization, metallophilic interactions, phase changes, and luminescence in four polymorphs of IrI(CO)2(OC(CH3)CHC(CH3)N(p-tol)).

Inorganic chemistry

Gussenhoven EM, Olmstead MM, Fettinger JC, Balch AL.
PMID: 18447342
Inorg Chem. 2008 Jun 02;47(11):4570-8. doi: 10.1021/ic702243z. Epub 2008 May 01.

Four polymorphs of IrI(CO)2(OC(CH3)CHC(CH3)N(p-tol)) have been characterized by single crystal X-ray crystallography. While all contain the same molecular unit with no significant structural variations within the molecules, all show different degrees of metallophilic interactions between the planar molecules. Three...

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Gussenhoven EM, Olmstead MM, Fettinger JC, et al. Interplay of supramolecular organization, metallophilic interactions, phase changes, and luminescence in four polymorphs of IrI(CO)2(OC(CH3)CHC(CH3)N(p-tol)). Inorg Chem. 2008;47(11):4570-8doi: 10.1021/ic702243z.
Gussenhoven, E. M., Olmstead, M. M., Fettinger, J. C., & Balch, A. L. (2008). Interplay of supramolecular organization, metallophilic interactions, phase changes, and luminescence in four polymorphs of IrI(CO)2(OC(CH3)CHC(CH3)N(p-tol)). Inorganic chemistry, 47(11), 4570-8. https://doi.org/10.1021/ic702243z
Gussenhoven, Emily M, et al. "Interplay of supramolecular organization, metallophilic interactions, phase changes, and luminescence in four polymorphs of IrI(CO)2(OC(CH3)CHC(CH3)N(p-tol))." Inorganic chemistry vol. 47,11 (2008): 4570-8. doi: https://doi.org/10.1021/ic702243z
Gussenhoven EM, Olmstead MM, Fettinger JC, Balch AL. Interplay of supramolecular organization, metallophilic interactions, phase changes, and luminescence in four polymorphs of IrI(CO)2(OC(CH3)CHC(CH3)N(p-tol)). Inorg Chem. 2008 Jun 02;47(11):4570-8. doi: 10.1021/ic702243z. Epub 2008 May 01. PMID: 18447342.
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