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Rhodium-catalyzed dehydrocoupling of the sterically encumbered phosphine-borane adduct tBu(2)PH.BH(3): synthesis of the linear dimers tBu(2)PH-BH(2)-tBu(2)P-BH(3) and tBu(2)PH-BH(2)-tBu(2)P-BH(2)Cl.

Inorganic chemistry

Dorn H, Vejzovic E, Lough AJ, Manners I.
PMID: 11487339
Inorg Chem. 2001 Aug 13;40(17):4327-31. doi: 10.1021/ic0100626.

The dehydrocoupling of the sterically hindered phosphine-borane adduct tBu(2)PH.BH(3) above 140 degrees C is catalyzed by the rhodium complexes [Rh(1,5-cod)(2)][OTf] or Rh(6)(CO)(16) to give the four-membered chain tBu(2)PH-BH(2)-tBu(2)P-BH(3) (1), which was isolated in 60% yield and characterized by multinuclear...

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Dorn H, Vejzovic E, Lough AJ, et al. Rhodium-catalyzed dehydrocoupling of the sterically encumbered phosphine-borane adduct tBu(2)PH.BH(3): synthesis of the linear dimers tBu(2)PH-BH(2)-tBu(2)P-BH(3) and tBu(2)PH-BH(2)-tBu(2)P-BH(2)Cl. Inorg Chem. 2001;40(17):4327-31doi: 10.1021/ic0100626.
Dorn, H., Vejzovic, E., Lough, A. J., & Manners, I. (2001). Rhodium-catalyzed dehydrocoupling of the sterically encumbered phosphine-borane adduct tBu(2)PH.BH(3): synthesis of the linear dimers tBu(2)PH-BH(2)-tBu(2)P-BH(3) and tBu(2)PH-BH(2)-tBu(2)P-BH(2)Cl. Inorganic chemistry, 40(17), 4327-31. https://doi.org/10.1021/ic0100626
Dorn, H, et al. "Rhodium-catalyzed dehydrocoupling of the sterically encumbered phosphine-borane adduct tBu(2)PH.BH(3): synthesis of the linear dimers tBu(2)PH-BH(2)-tBu(2)P-BH(3) and tBu(2)PH-BH(2)-tBu(2)P-BH(2)Cl." Inorganic chemistry vol. 40,17 (2001): 4327-31. doi: https://doi.org/10.1021/ic0100626
Dorn H, Vejzovic E, Lough AJ, Manners I. Rhodium-catalyzed dehydrocoupling of the sterically encumbered phosphine-borane adduct tBu(2)PH.BH(3): synthesis of the linear dimers tBu(2)PH-BH(2)-tBu(2)P-BH(3) and tBu(2)PH-BH(2)-tBu(2)P-BH(2)Cl. Inorg Chem. 2001 Aug 13;40(17):4327-31. doi: 10.1021/ic0100626. PMID: 11487339.
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Hydrated salts of 3,5-dihydroxybenzoic acid with organic diamines: hydrogen-bonded supramolecular structures in two and three dimensions.

Acta crystallographica. Section B, Structural science

Burchell CJ, Ferguson G, Lough AJ, Gregson RM, Glidewell C.
PMID: 11373391
Acta Crystallogr B. 2001 Jun;57:329-38. doi: 10.1107/s0108768100019832. Epub 2001 Jun 01.

The trigonally trisubstituted acid 3,5-dihydroxybenzoic acid forms hydrated salt-type adducts with organic diamines. In 1,4-diazabicyclo[2.2.2]octane-3,5-dihydroxybenzoic acid-water (1/1/1) (1), where Z' = 2 in P2(1)/c, the constitution is [HN(CH(2)CH(2))(3)N](+).[(HO)(2)C(6)H(3)COO](-).H(2)O: the anions and the water molecules are linked by six O-H.O...

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Burchell CJ, Ferguson G, Lough AJ, et al. Hydrated salts of 3,5-dihydroxybenzoic acid with organic diamines: hydrogen-bonded supramolecular structures in two and three dimensions. Acta Crystallogr B. 2001;57:329-38doi: 10.1107/s0108768100019832.
Burchell, C. J., Ferguson, G., Lough, A. J., Gregson, R. M., & Glidewell, C. (2001). Hydrated salts of 3,5-dihydroxybenzoic acid with organic diamines: hydrogen-bonded supramolecular structures in two and three dimensions. Acta crystallographica. Section B, Structural science, 57329-38. https://doi.org/10.1107/s0108768100019832
Burchell, C J, et al. "Hydrated salts of 3,5-dihydroxybenzoic acid with organic diamines: hydrogen-bonded supramolecular structures in two and three dimensions." Acta crystallographica. Section B, Structural science vol. 57 (2001): 329-38. doi: https://doi.org/10.1107/s0108768100019832
Burchell CJ, Ferguson G, Lough AJ, Gregson RM, Glidewell C. Hydrated salts of 3,5-dihydroxybenzoic acid with organic diamines: hydrogen-bonded supramolecular structures in two and three dimensions. Acta Crystallogr B. 2001 Jun;57:329-38. doi: 10.1107/s0108768100019832. Epub 2001 Jun 01. PMID: 11373391.
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Phosphonopropionic acid as a building block in supramolecular chemistry: salts with organic diamines.

Acta crystallographica. Section B, Structural science

Bowes KF, Ferguson G, Lough AJ, Glidewell C.
PMID: 12657817
Acta Crystallogr B. 2003 Apr;59:248-62. doi: 10.1107/s0108768102021237. Epub 2003 Mar 26.

The structures of seven salts formed by phosphonopropionic acid with organic diamines are reported; in these salts, the hydrogen-bonded substructures formed by the anions can be zero-, one- or two-dimensional, while the overall hydrogen-bonded supramolecular structures are three-dimensional. The...

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Bowes KF, Ferguson G, Lough AJ, et al. Phosphonopropionic acid as a building block in supramolecular chemistry: salts with organic diamines. Acta Crystallogr B. 2003;59:248-62doi: 10.1107/s0108768102021237.
Bowes, K. F., Ferguson, G., Lough, A. J., & Glidewell, C. (2003). Phosphonopropionic acid as a building block in supramolecular chemistry: salts with organic diamines. Acta crystallographica. Section B, Structural science, 59248-62. https://doi.org/10.1107/s0108768102021237
Bowes, Katharine F, et al. "Phosphonopropionic acid as a building block in supramolecular chemistry: salts with organic diamines." Acta crystallographica. Section B, Structural science vol. 59 (2003): 248-62. doi: https://doi.org/10.1107/s0108768102021237
Bowes KF, Ferguson G, Lough AJ, Glidewell C. Phosphonopropionic acid as a building block in supramolecular chemistry: salts with organic diamines. Acta Crystallogr B. 2003 Apr;59:248-62. doi: 10.1107/s0108768102021237. Epub 2003 Mar 26. PMID: 12657817.
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Preparation of Rhenium(I) and Rhenium(II) Amine Dinitrogen Complexes and the Characterization of an Elongated Dihydrogen Species.

Inorganic chemistry

Chin RM, Barrera J, Dubois RH, Helberg LE, Sabat M, Bartucz TY, Lough AJ, Morris RH, Harman WD.
PMID: 11670037
Inorg Chem. 1997 Jul 30;36(16):3553-3558. doi: 10.1021/ic9700866.

A series of rhenium(I) dinitrogen complexes were prepared containing predominantly amine ligands. On the basis of infrared and electrochemical data, a system was selected that was anticipated to be a suitable precursor for an elongated dihydrogen complex. Upon oxidation...

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Chin RM, Barrera J, Dubois RH, et al. Preparation of Rhenium(I) and Rhenium(II) Amine Dinitrogen Complexes and the Characterization of an Elongated Dihydrogen Species. Inorg Chem. 1997;36(16):3553-3558doi: 10.1021/ic9700866.
Chin, R. M., Barrera, J., Dubois, R. H., Helberg, L. E., Sabat, M., Bartucz, T. Y., Lough, A. J., Morris, R. H., & Harman, W. D. (1997). Preparation of Rhenium(I) and Rhenium(II) Amine Dinitrogen Complexes and the Characterization of an Elongated Dihydrogen Species. Inorganic chemistry, 36(16), 3553-3558. https://doi.org/10.1021/ic9700866
Chin, R. Martin, et al. "Preparation of Rhenium(I) and Rhenium(II) Amine Dinitrogen Complexes and the Characterization of an Elongated Dihydrogen Species." Inorganic chemistry vol. 36,16 (1997): 3553-3558. doi: https://doi.org/10.1021/ic9700866
Chin RM, Barrera J, Dubois RH, Helberg LE, Sabat M, Bartucz TY, Lough AJ, Morris RH, Harman WD. Preparation of Rhenium(I) and Rhenium(II) Amine Dinitrogen Complexes and the Characterization of an Elongated Dihydrogen Species. Inorg Chem. 1997 Jul 30;36(16):3553-3558. doi: 10.1021/ic9700866. PMID: 11670037.
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F8BINOL, an electronically perturbed version of BINOL with remarkable configurational stability.

Organic letters

Yudin AK, Martyn LJ, Pandiaraju S, Zheng J, Lough A.
PMID: 10814241
Org Lett. 2000 Jan;2(1):41-4. doi: 10.1021/ol991244v.

[structure: see text] Substitution of hydrogens by fluorines at the 5, 5', 6, 6', 7, 7', 8, and 8' positions of BINOL strongly affects distribution of electron density within the biaryl skeleton but has a very small influence on...

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Yudin AK, Martyn LJ, Pandiaraju S, et al. F8BINOL, an electronically perturbed version of BINOL with remarkable configurational stability. Org Lett. 2000;2(1):41-4doi: 10.1021/ol991244v.
Yudin, A. K., Martyn, L. J., Pandiaraju, S., Zheng, J., & Lough, A. (2000). F8BINOL, an electronically perturbed version of BINOL with remarkable configurational stability. Organic letters, 2(1), 41-4. https://doi.org/10.1021/ol991244v
Yudin, et al. "F8BINOL, an electronically perturbed version of BINOL with remarkable configurational stability." Organic letters vol. 2,1 (2000): 41-4. doi: https://doi.org/10.1021/ol991244v
Yudin AK, Martyn LJ, Pandiaraju S, Zheng J, Lough A. F8BINOL, an electronically perturbed version of BINOL with remarkable configurational stability. Org Lett. 2000 Jan;2(1):41-4. doi: 10.1021/ol991244v. PMID: 10814241.
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Rethinking the formula.

Drug discovery today

Clough J.
PMID: 11983566
Drug Discov Today. 2002 May 01;7(9):506-8. doi: 10.1016/s1359-6446(02)02276-6.

No abstract available.

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Clough J. Rethinking the formula. Drug Discov Today. 2002;7(9):506-8doi: 10.1016/s1359-6446(02)02276-6.
Clough, J. (2002). Rethinking the formula. Drug discovery today, 7(9), 506-8. https://doi.org/10.1016/s1359-6446(02)02276-6
Clough, Joanne. "Rethinking the formula." Drug discovery today vol. 7,9 (2002): 506-8. doi: https://doi.org/10.1016/s1359-6446(02)02276-6
Clough J. Rethinking the formula. Drug Discov Today. 2002 May 01;7(9):506-8. doi: 10.1016/s1359-6446(02)02276-6. PMID: 11983566.
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Self-assembled hydrogen-bonded bilayers in 1,4-diazabicyclo[2.2.2]octane-N-(phosphonomethyl)iminodiacetic acid-water (1/1/1.5).

Acta crystallographica. Section C, Crystal structure communications

Bowes KF, Ferguson G, Glidewell C, Lough AJ.
PMID: 12154301
Acta Crystallogr C. 2002 Aug;58:o467-9. doi: 10.1107/s0108270102010648. Epub 2002 Jul 12.

The title compound is a hydrated salt, 1,4-diazoniabicyclo[2.2.2]octane-N-[(hydroxyphosphinato)methyl]iminiodiacetate-water (1/1/1.5), C(6)H(14)N(2)(2+).C(5)H(8)NO(7)P(2-).1.5H(2)O, in which one of the water molecules lies across a twofold rotation axis in space group P2/n. The ionic components are linked into sheets by a combination of a...

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Bowes KF, Ferguson G, Glidewell C, et al. Self-assembled hydrogen-bonded bilayers in 1,4-diazabicyclo[2.2.2]octane-N-(phosphonomethyl)iminodiacetic acid-water (1/1/1.5). Acta Crystallogr C. 2002;58:o467-9doi: 10.1107/s0108270102010648.
Bowes, K. F., Ferguson, G., Glidewell, C., & Lough, A. J. (2002). Self-assembled hydrogen-bonded bilayers in 1,4-diazabicyclo[2.2.2]octane-N-(phosphonomethyl)iminodiacetic acid-water (1/1/1.5). Acta crystallographica. Section C, Crystal structure communications, 58o467-9. https://doi.org/10.1107/s0108270102010648
Bowes, Katharine F, et al. "Self-assembled hydrogen-bonded bilayers in 1,4-diazabicyclo[2.2.2]octane-N-(phosphonomethyl)iminodiacetic acid-water (1/1/1.5)." Acta crystallographica. Section C, Crystal structure communications vol. 58 (2002): o467-9. doi: https://doi.org/10.1107/s0108270102010648
Bowes KF, Ferguson G, Glidewell C, Lough AJ. Self-assembled hydrogen-bonded bilayers in 1,4-diazabicyclo[2.2.2]octane-N-(phosphonomethyl)iminodiacetic acid-water (1/1/1.5). Acta Crystallogr C. 2002 Aug;58:o467-9. doi: 10.1107/s0108270102010648. Epub 2002 Jul 12. PMID: 12154301.
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Left-sided multifractality in a binary random multiplicative cascade.

Physical review. E, Statistical, nonlinear, and soft matter physics

Hanan WG, Gough J, Heffernan DM.
PMID: 11304236
Phys Rev E Stat Nonlin Soft Matter Phys. 2001 Jan;63(1):011109. doi: 10.1103/PhysRevE.63.011109. Epub 2000 Dec 27.

In this paper we study a binary random multiplicative cascade. Specifically, the cascade is used to produce and study left-sided multifractal random measures. Extensive numerical simulations of the random cascade process were undertaken and f(alpha) spectra obtained and compared...

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Hanan WG, Gough J, Heffernan DM. Left-sided multifractality in a binary random multiplicative cascade. Phys Rev E Stat Nonlin Soft Matter Phys. 2000;63(1):011109doi: 10.1103/PhysRevE.63.011109.
Hanan, W. G., Gough, J., & Heffernan, D. M. (2001). Left-sided multifractality in a binary random multiplicative cascade. Physical review. E, Statistical, nonlinear, and soft matter physics, 63(1), 011109. https://doi.org/10.1103/PhysRevE.63.011109
Hanan, W G, et al. "Left-sided multifractality in a binary random multiplicative cascade." Physical review. E, Statistical, nonlinear, and soft matter physics vol. 63,1 (2001): 011109. doi: https://doi.org/10.1103/PhysRevE.63.011109
Hanan WG, Gough J, Heffernan DM. Left-sided multifractality in a binary random multiplicative cascade. Phys Rev E Stat Nonlin Soft Matter Phys. 2001 Jan;63(1):011109. doi: 10.1103/PhysRevE.63.011109. Epub 2000 Dec 27. PMID: 11304236.
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Mechanism of the hydrogenation of ketones catalyzed by trans-dihydrido(diamine)ruthenium II complexes.

Journal of the American Chemical Society

Abdur-Rashid K, Clapham SE, Hadzovic A, Harvey JN, Lough AJ, Morris RH.
PMID: 12475357
J Am Chem Soc. 2002 Dec 18;124(50):15104-18. doi: 10.1021/ja016817p.

The complexes trans-RuH(Cl)(tmen)(R-binap) (1) and (OC-6-43)-RuH(Cl)(tmen)(PPh(3))(2) (2) are prepared by the reaction of the diamine NH(2)CMe(2)CMe(2)NH(2) (tmen) with RuH(Cl)(PPh(3))(R-binap) and RuH(Cl)(PPh(3))(3), respectively. Reaction of KHB(sec)Bu(3) with 1 yields trans-Ru(H)(2)(R-binap)(tmen) (5) while reaction of KHB(sec)Bu(3) or KO(t)Bu with 2 under...

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Abdur-Rashid K, Clapham SE, Hadzovic A, et al. Mechanism of the hydrogenation of ketones catalyzed by trans-dihydrido(diamine)ruthenium II complexes. J Am Chem Soc. 2002;124(50):15104-18doi: 10.1021/ja016817p.
Abdur-Rashid, K., Clapham, S. E., Hadzovic, A., Harvey, J. N., Lough, A. J., & Morris, R. H. (2002). Mechanism of the hydrogenation of ketones catalyzed by trans-dihydrido(diamine)ruthenium II complexes. Journal of the American Chemical Society, 124(50), 15104-18. https://doi.org/10.1021/ja016817p
Abdur-Rashid, Kamaluddin, et al. "Mechanism of the hydrogenation of ketones catalyzed by trans-dihydrido(diamine)ruthenium II complexes." Journal of the American Chemical Society vol. 124,50 (2002): 15104-18. doi: https://doi.org/10.1021/ja016817p
Abdur-Rashid K, Clapham SE, Hadzovic A, Harvey JN, Lough AJ, Morris RH. Mechanism of the hydrogenation of ketones catalyzed by trans-dihydrido(diamine)ruthenium II complexes. J Am Chem Soc. 2002 Dec 18;124(50):15104-18. doi: 10.1021/ja016817p. PMID: 12475357.
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meso-5,5,7,12,12,14-hexamethyl-1,4-diaza-8,11-diazoniacyclotetradecane bis(2-naphthoate) ethanol disolvate: centrosymmetric five-component aggregates linked into sheets by C-H...pi(arene) hydrogen bonding.

Acta crystallographica. Section C, Crystal structure communications

Bowes KF, Ferguson G, Lough AJ, Glidewell C.
PMID: 12711791
Acta Crystallogr C. 2003 Mar;59:o147-9. doi: 10.1107/s0108270103002804. Epub 2003 Feb 18.

The title compound is an ethanol-solvated salt, C(16)H(38)N(4)(2+) x -2C(11)H(7)O(2)(-) x -2C(2)H(6)O, in which the cation lies across a centre of inversion in P2(1)/c. The ions are linked by N-H...O hydrogen bonds [H...O = 1.70 and 2.30 A, N...O...

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Bowes KF, Ferguson G, Lough AJ, et al. meso-5,5,7,12,12,14-hexamethyl-1,4-diaza-8,11-diazoniacyclotetradecane bis(2-naphthoate) ethanol disolvate: centrosymmetric five-component aggregates linked into sheets by C-H...pi(arene) hydrogen bonding. Acta Crystallogr C. 2003;59:o147-9doi: 10.1107/s0108270103002804.
Bowes, K. F., Ferguson, G., Lough, A. J., & Glidewell, C. (2003). meso-5,5,7,12,12,14-hexamethyl-1,4-diaza-8,11-diazoniacyclotetradecane bis(2-naphthoate) ethanol disolvate: centrosymmetric five-component aggregates linked into sheets by C-H...pi(arene) hydrogen bonding. Acta crystallographica. Section C, Crystal structure communications, 59o147-9. https://doi.org/10.1107/s0108270103002804
Bowes, Katharine F, et al. "meso-5,5,7,12,12,14-hexamethyl-1,4-diaza-8,11-diazoniacyclotetradecane bis(2-naphthoate) ethanol disolvate: centrosymmetric five-component aggregates linked into sheets by C-H...pi(arene) hydrogen bonding." Acta crystallographica. Section C, Crystal structure communications vol. 59 (2003): o147-9. doi: https://doi.org/10.1107/s0108270103002804
Bowes KF, Ferguson G, Lough AJ, Glidewell C. meso-5,5,7,12,12,14-hexamethyl-1,4-diaza-8,11-diazoniacyclotetradecane bis(2-naphthoate) ethanol disolvate: centrosymmetric five-component aggregates linked into sheets by C-H...pi(arene) hydrogen bonding. Acta Crystallogr C. 2003 Mar;59:o147-9. doi: 10.1107/s0108270103002804. Epub 2003 Feb 18. PMID: 12711791.
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Threefold interweaving of (4,4) nets built from R(10)10(58) rings inthe hydrogen-bonded adduct 1,4-diazabicyclo.

Acta crystallographica. Section C, Crystal structure communications

Burchell CJ, Ferguson G, Lough AJ, Glidewell C.
PMID: 10986506
Acta Crystallogr C. 2000 Sep;56:1126-8. doi: 10.1107/s010827010000771x.

The 1:1 adduct of 1,4-diazabicyclo[2.2.2]octane and 5-hydroxyisophthalic acid is a salt, [H(C(6)H(12)N(2))](+). [HOC(6)H(3)(COOH)COO](-) or C(6)H(13)N(2)(+).C(8)H(5)O(5)(-). The ions are linked by three types of hydrogen bond, i.e. N-H.O, O-H.O and O-H.N, into continuous two-dimensional (4,4) nets built from a single...

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Burchell CJ, Ferguson G, Lough AJ, et al. Threefold interweaving of (4,4) nets built from R(10)10(58) rings inthe hydrogen-bonded adduct 1,4-diazabicyclo. Acta Crystallogr C. 2000;56:1126-8doi: 10.1107/s010827010000771x.
Burchell, C. J., Ferguson, G., Lough, A. J., & Glidewell, C. (2000). Threefold interweaving of (4,4) nets built from R(10)10(58) rings inthe hydrogen-bonded adduct 1,4-diazabicyclo. Acta crystallographica. Section C, Crystal structure communications, 561126-8. https://doi.org/10.1107/s010827010000771x
Burchell, et al. "Threefold interweaving of (4,4) nets built from R(10)10(58) rings inthe hydrogen-bonded adduct 1,4-diazabicyclo." Acta crystallographica. Section C, Crystal structure communications vol. 56 (2000): 1126-8. doi: https://doi.org/10.1107/s010827010000771x
Burchell CJ, Ferguson G, Lough AJ, Glidewell C. Threefold interweaving of (4,4) nets built from R(10)10(58) rings inthe hydrogen-bonded adduct 1,4-diazabicyclo. Acta Crystallogr C. 2000 Sep;56:1126-8. doi: 10.1107/s010827010000771x. PMID: 10986506.
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Carbamoyl-substituted N-heterocyclic carbene complexes of palladium(II): application to Sonogashira cross-coupling reactions.

Organic letters

Batey RA, Shen M, Lough AJ.
PMID: 11975591
Org Lett. 2002 May 02;4(9):1411-4. doi: 10.1021/ol017245g.

[reaction: see text]. The first examples of N-carbamoyl-substituted heterocyclic carbene Pd(II) complexes are described. These thermal and hydrolytically stable complexes are readily prepared from carbamoyl imidazolium salts and efficiently promote Sonogashira cross-coupling reactions under mild conditions. Cesium carbonate is...

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Batey RA, Shen M, Lough AJ. Carbamoyl-substituted N-heterocyclic carbene complexes of palladium(II): application to Sonogashira cross-coupling reactions. Org Lett. 2002;4(9):1411-4doi: 10.1021/ol017245g.
Batey, R. A., Shen, M., & Lough, A. J. (2002). Carbamoyl-substituted N-heterocyclic carbene complexes of palladium(II): application to Sonogashira cross-coupling reactions. Organic letters, 4(9), 1411-4. https://doi.org/10.1021/ol017245g
Batey, Robert A, et al. "Carbamoyl-substituted N-heterocyclic carbene complexes of palladium(II): application to Sonogashira cross-coupling reactions." Organic letters vol. 4,9 (2002): 1411-4. doi: https://doi.org/10.1021/ol017245g
Batey RA, Shen M, Lough AJ. Carbamoyl-substituted N-heterocyclic carbene complexes of palladium(II): application to Sonogashira cross-coupling reactions. Org Lett. 2002 May 02;4(9):1411-4. doi: 10.1021/ol017245g. PMID: 11975591.
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