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Showing 25 to 36 of 1439 entries
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Flow injection chemiluminescent method for the successive determination of l-cysteine and l-cystine using photogenerated tris(2,2'-bipyridyl) ruthenium (III).

Talanta

Pérez-Ruiz T, Martínez-Lozano C, Tomás V, Martín J.
PMID: 18968832
Talanta. 2002 Nov 12;58(5):987-94.

Flow injection configurations were developed for the individual determination of l-cysteine and l-cystine and for the mixture of both analytes. The method is based on the reaction of l-cysteine with tris(2,2'-bipyridyl) ruthenium (II) and peroxydisulphate under UV irradiation to...

A sensitive and selective spectrophotometric estimation of catechol derivatives in pharmaceutical preparations.

Talanta

Nagaraja P, Vasantha RA, Sunitha KR.
PMID: 18968454
Talanta. 2001 Dec 24;55(6):1039-46. doi: 10.1016/s0039-9140(01)00438-6.

A sensitive and simple spectrophotometric method for the estimation of catechol and its derivatives like dopamine hydrochloride (DPH), levodopa (LDP), methyldopa (MDP) and adrenaline hydrochloride (ADH) in both pure form and in pharmaceutical formulation, is described. The method is...

Spectrofluorimetric study of the beta-cyclodextrin-rubidate complex and determination of rubidate by beta-CD-enhanced fluorimetry.

Talanta

Tang B, Ma L, Ma C.
PMID: 18968814
Talanta. 2002 Nov 12;58(5):841-8. doi: 10.1016/s0039-9140(02)00400-9.

The supramolecular interaction of rubidate (chemically 2,3-naphthalenedicarboxylic acid, 1,4-dihydroxy-diethyl ester) and beta-cyclodextrin (beta-CD) has been studied by spectrofluorimetry. The influence of temperature on the supramolecular system has also been investigated and the thermodynamic parameters were calculated. The results show...

Determination of thiamine by continuous flow chemiluminescence measurement.

Talanta

Grekas N, Calokerinos AC.
PMID: 18965066
Talanta. 1990 Nov;37(11):1043-8. doi: 10.1016/0039-9140(90)80151-5.

The chemiluminescence produced by oxidation of thiamine by ferricyanide in alkaline medium has been investigated by using a simple continuous flow analyser and a procedure developed for the determination of thiamine hydrochloride or nitrate in the range 2.00 x...

Kinetic study of the determination of hydrazines, isoniazid and sodium azide by monitoring their reactions with 1-fluoro-2,4-dinitrobenzene, by means of a fluoride-selective electrode.

Talanta

Athanasiou-Malaki E, Koupparis MA.
PMID: 18964734
Talanta. 1989 Apr;36(4):431-6. doi: 10.1016/0039-9140(89)80224-3.

A kinetic potentiometric method is described for the determination of hydrazines (hydrazine, phenylhydrazine, hydralazine and procarbazine), isoniazid and sodium azide, based on monitoring their reactions at 25 degrees and pH 9.0 with 1-fluoro-2,4-dinitrobenzene by means of a fluoride-selective electrode....

Determination of ascorbic acid in pharmaceutical preparations by near infrared reflectance spectroscopy.

Talanta

Blanco M, Coello J, Iturriaga H, Maspoch S, de la Pezuela C.
PMID: 18965838
Talanta. 1993 Nov;40(11):1671-6. doi: 10.1016/0039-9140(93)80083-4.

We developed a method for determination of ascorbic acid in pharmaceutical preparations containing various excipients by using near infrared diffuse reflectance spectroscopy and two different calibration methods, viz. stepwise multiple linear regression (SMLR) and partial least-squares (PLS) regression, which...

Determination of pentoxifylline in pharmaceutical formulations using iodine as oxidizing agent.

Talanta

Sastry CS, Naidu PY.
PMID: 18967264
Talanta. 1998 Aug;46(6):1357-62. doi: 10.1016/s0039-9140(98)00003-4.

Simple, selective and sensitive spectrophotometric methods are described for the determination of pentoxifylline, based on the haloform reaction with a known and excess of standard iodine solution under alkaline conditions. The excess of iodine is determined at pH 3.0...

Determination of bromhexine in cough-cold syrups by absorption spectrophotometry and multivariate calibration using partial least-squares and hybrid linear analyses. Application of a novel method of wavelength selection.

Talanta

Goicoechea HC, Olivieri AC.
PMID: 18967655
Talanta. 1999 Jul 12;49(4):793-800. doi: 10.1016/s0039-9140(99)00080-6.

The mucolitic bromhexine [N-(2-amino-3,5-dibromobenzyl)-N-methylcyclohexylamine] has been determined in cough suppressant syrups by multivariate spectrophotometric calibration, together with partial least-squares (PLS-1) and hybrid linear analysis (HLA). Notwithstanding the spectral overlapping between bromhexine and syrup excipients, as well as the intrinsic...

Electrochemical reduction of nicergoline and its analytical determination in dosage forms.

Talanta

Sturm JC, Nunez-Vergara LJ, Squella JA.
PMID: 18965506
Talanta. 1992 Sep;39(9):1149-54. doi: 10.1016/0039-9140(92)80213-w.

Electrochemical reduction of nicergoline was studied at different pH and concentrations using differential pulse polarography and linear sweep voltammetry. Both techniques reveal that the reduction process occurs with strong adsorption of the product. Nicergoline is an excellent model for...

Development and evaluation of hepatoprotective polyherbal formulation containing some indigenous medicinal plants.

Indian journal of pharmaceutical sciences

Dandagi PM, Patil MB, Mastiholimath VS, Gadad AP, Dhumansure RH.
PMID: 20046731
Indian J Pharm Sci. 2008 Mar-Apr;70(2):265-8. doi: 10.4103/0250-474X.41474.

The present study explores the hepatoprotective activity of various extracts of Ferula asafoetida, Momordica charantia Linn and Nardostachys jatamansi against experimental hepatotoxicity. Polyherbal suspensions were formulated using extracts showing significant activity and evaluated for both physicochemical and hepatoprotective activity...

Simultaneous derivative spectrophotometric analysis of doxylamine succinate, pyridoxine hydrochloride and folic Acid in combined dosage forms.

Indian journal of pharmaceutical sciences

Pathak A, Rajput SJ.
PMID: 20046784
Indian J Pharm Sci. 2008 Jul-Aug;70(4):513-7. doi: 10.4103/0250-474X.44607.

Two UV spectrophotometric methods have been developed, based on first derivative spectrophotometry for simultaneous estimation of doxylamine succinate, pyridoxine hydrochloride, and folic acid in tablet formulations. In method I, the concentrations of these drugs were determined by using linear...

Development of a novel liquid chromatography--evaporative light scattering detection method for bacitracins and applications to quality control of pharmaceuticals.

Analytica chimica acta

Sarri AK, Megoulas NC, Koupparis MA.
PMID: 17723531
Anal Chim Acta. 2006 Jul 28;573:250-7. doi: 10.1016/j.aca.2006.05.042. Epub 2006 May 20.

A novel liquid chromatography method for the direct determination of bacitracin main components (Bc-A, -B1, -B2 and -B3), a basic, cyclic polypeptide antibiotic, was developed and validated, based on ion pairs formation with trifluoroacetic acid (TFA) and evaporative light...

Showing 25 to 36 of 1439 entries